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薄层扫描法测定咳安含片中西贝碱的含量
http://www.100md.com 《时珍国医国药》 2006年第6期
咳安含片;,西贝碱;,薄层扫描法,,咳安含片;,西贝碱;,薄层扫描法,摘要,关键词,1仪器与试剂,2方法与结果,3小结,参考文献
     摘要:目的研究咳安含片中西贝碱的含量测定。方法采用薄层扫描法进行测定。结果西贝碱在0.26~1.60 μg之间线性关系良好,相关系数R=0.999 8,回收率为95.60%,RSD为1.60%。结论 该法灵敏、简便、准确,可用于该制剂的测定和质量控制指标。

    关键词:咳安含片; 西贝碱; 薄层扫描法

    TLC Scanning for the Determination of Imperialine in Kean Buccal Tablets

    LIU Wei,SONG Weizhong, SONG Xiaoyong

    (1.Dongjing Hospital of Henan University , Kaifeng 475001, China; 2.Henan University ,Henan Kaifeng 475001, China)

    Abstract:ObjectiveTo develop an assay for the quantitative determination of imperialine in Kean buccal Tablets. MethodsTLCS method was selected to determine the content.ResultsThe linearity was obtained over the range of 0.26~1.60 μg(r=0.999 8).The average recovery was 95.60%, RSD was 1.60%.ConclusionThe results showed that this method was sensitive,simple,sepecific and accurate for the determination of imperialine in Kean buccal tablets.

    Key words:Kean buccal tablets; Imperialine; TLC

    咳安含片是由川贝母、枇杷叶、桔梗、薄荷脑组成的方剂 ......

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